Hi there Patrick,
It sounds like you had fun getting into the details of your engine build! I hope it goes well for you.
I would like to see a bit more accuracy in the measurements. A flat piece of perspex on the head with small hole and the use of highly accurate burette (which do not cost a bomb anyhow) will give better chamber cc results. You need to know the exact cc's of your own particular cylinder head chambers.
The liquid could do well to be either alcohol with a dye or a very fine llightweight oil as water's surface tension can be an issue.
The method of placing head gasket on the head and pushing piston into the chamber I believe will not give very accurate TDC chamber volume as there are too many variables... For pistons with material protruding from the top of the bore it is a little more complex to measure than those which can have the perspex and burette technique applied. Piston specifications from the manufacturer and commonly available internet calculators will give adequate results and also take the varying head gasket thicknesses available into consideration very easily.
I do like your method of tipping in the final cc's worth of dyed liquid into the chamber to mark the amount to be milled - rather resourseful!
Cheers,
Jason
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